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2019006133

CERTIFICATE OF ANALYSIS
QUALITY CONTROL PERFORMANCE REPORT

PRODUCT INFORMATION

SERIAL NUMBER : 2019006133

PART NUMBER : S8034-034360
PRODUCT TYPE : ChraSep SPE Columns ODS-IC 500mg/3ml, 50/pk
LOT : 639753201

 

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RAW MATERIALS
Component Properties
Properties Specifications Results Methods
Tube Purity Proprietary Pass GC FID Test
Frit Purity Proprietary Pass GC FID Test
Base Silica Physical Properties
Properties Specifications Results Methods
Surface Area (m2/g) 450-550 535 N2 BET
Particle Size (µm) 45-60 46 Malvern 100
Pore Diameter (Å) 60-90   N2 BET
Particle Size Distribution (%) ≤20µm ≤ 35µm ≥80µm ≤20µm ≤ 35µm ≥80µm Malvern 100
  ≤ 11 ≤18 ≤15 ≤ 8 ≤15 ≤10  
PRODUCT SPECIFICATION/ANALYSIS
Bonded Silica Properties
Properties Specifications Results Methods
Carbon Loading (%C) 17.0-20.0 19.5 CHNO-S Analysis
Hydrogen Loading(%H) 1.5-6.0 3.95 CHNO-S Analysis
Surface Coverage (µmol/m2) 1.90-2.50 2.05 Calculated based on %C
Turbidity (NTU) ≤10.0 0.55 Turbidity meter
Washable Residue (mg/g) ≤2.0 0.2 Methanol and Hexane gravimetric
Bed Mass Consistency Proprietary Pass Weight Measurement
Flow Characteristics Proprietary Pass Methanol in low vacuum (1” Hg)
HPLC Test Conditions
Column Dimension 100 x 4.6 mm
Flow 1 mL/min
Detector UV@254 nm
Mobile Phase Methanol:Water (60:40)
Temperature 25-35 oC
Probes Uracil, Acetophenone, Nitrobenzene, Benzene, Toluene
MATERIAL SAFETY DATA SHEETS ARE AVAILABLE UPON REQUEST
ChraReport at https://chracert.com/2019006133